Please note: If you switch to a different device, you may be asked to login again with only your ACS ID. h�bbd```b``���@$�0[D2��H�G`�i �UL��e���4��u�E l&X�,����sg�mi��kA$X�l�$�%� ���l/��} ��f4��l�6 ���g&����a`��&�� ;F� endobj Clicking on the donut icon will load a page at with additional details about the score and the social media presence for the given article. Abstract The extraction efficiency of Soxhlet, acid hydrolysis and Bligh and Dyer were evaluated by using direct methylation on extracts and residues for calculating the mass balance of fatty acids for eight marine powders (fishmeals, krillmeals, cod filet, salmon filet Chang. 13 publications. Physicochemical properties and storage stability of soybean protein nanoemulsions prepared by ultra-high pressure homogenization. Page 1 of 1 F419 Crude Fat (Acid Hydrolysis) Samples containing complexed/bound lipids or fats (e.g. You have to login with your ACS ID befor you can login with your Mendeley account. You’ve supercharged your research process with ACS and Mendeley! Kubendran Devaraj, Salma Aathika, Yuvarai Mani, Amudha Thanarasu, Karthik Periyasamy, Premkumar Periyaraman, Karthikeyan Velayutham, Sivanesan Subramanian. Siu-Leung Chau, Ho-Wai Tang, Yu-Hong Cheng, Chun-Nam Lok, and Kwan-Ming Ng . acid hydrolysis) before extraction and quantifying the total crude fat content. According to Joslyn (1970) , the extracted fat percentage of dried egg, flour, noodles, and semolina was increased by 1–6% due to pre acid digestion. endobj Your Mendeley pairing has expired. '���ɼ,�&۾]^�L2��T*�X�D2�d"$[��/��MS��{���� s��jy��T�"-����-�����J&�,�+LJ��g1��e9��)˔ʒ4;��zE)�]^�ä8��Ce@�,��!&7����a�e?�sY�Q�[��3+ A��k�x]�Y�K�5^�~�U���[x�F�phq}���Y�SF@QJ>�ӑO�>)0*��TB6�����!+����x�^���`��l����>V��z �Q����l�)��ϸ���>�������l��?��y��?r����ۓ��Q�l@�D?��v�� ��y���'r�g�L�TbOhH��X�Rhg��SIb}VIe|��?99��UF��(. +%v����QN��S�#���f?3;�۳�I_S�cS��ώ�������Z�]W�MC?�c!��>/8^��h���֗�����ʗ�+�"2�A��&�2���&Y�P#�R������E��%���#��Rg- �d�����N�q��\M�$�H����n7��'R����B���L�m[]����c8k S-��}�ݾA�W Extraction and Liquid Chromatography–Tandem Mass Spectrometry Detection of 3-Monochloropropanediol Esters and Glycidyl Esters in Infant Formula. %PDF-1.6 %����,,,,,,,,, Chemical Printing of Biological Tissue by Gold Nanoparticle-Assisted Laser Ablation. %PDF-1.5 Fat Extraction from Acid- and Base-Hydrolyzed Food Samples Using Accelerated Solvent Extraction, Dionex Corporation, 445 Lakeside Drive, Sunnyvale, California 94085, United States, SLC Technical Center, Dionex Corporation, Suite A, 1182 West 2400 South, Salt Lake City, Utah 84119, United States. It is difficult to pursue direct ASE with acid- or base-hydrolyzed samples due to the corrosive nature of the reagents and material limitations. The acid hydrolysis method is applicable to baked products and pet foods, and facilitates the extraction of fatty acids from glycerides, glycolipids and phospholipids and sterol esters that might otherwise be left un-extracted due to covalent and ionic bonding. Response Surface Modeling and Optimization of Accelerated Solvent Extraction of Four Lignans from Fructus Schisandrae. The Altmetric Attention Score is a quantitative measure of the attention that a research article has received online. fat extraction acid hydrolysis base hydrolysis gravimetry fat analysis sample preparation Cited By This article is cited by 12 publications. The performance data are presented here for the new methods for lipid extraction for a variety of food samples and compared to the Mojonnier method. Application Note 361 Extraction of Total Fat from Food Samples After Acid Hydrolysis Using Accelerated Solvent Extraction (ASE) with GC-MS Analysis IntroductIon Sample preparation—specifically, solvent extraction—is an important step in the analytical process. stream Analysis of omega-3 fatty acids in foods and supplements. Article Views are the COUNTER-compliant sum of full text article downloads since November 2008 (both PDF and HTML) across all institutions and individuals. 4 Soxhlet extraction Vs Acid hydrolysis GB/T 5009.6-2003 Determination of fat in foods ¾Soxhlet extraction Crude fat including free fat (듥싷꿗 )¾Acid hydrolysis Total fat including free and bounded fat … I�]���5o�>8���ة���o�3�"e+�6d����͈l���{7�x��{��5�~��?�ls���lsy��Y��UU�)�%�^���������#l����~���U�/W͚}�_��~������S3��ܴ�e��w���w=.-�������ˋ���L$�b���@ baked and extruded products and pet foods) require acid to breakdown the fats (e.g. z@#�=O}�6O� ���*���;�OK$�١ q���oC#�br&��Td�lHD�#B ��X)X(�i������pʕhӦf��Jp&. NIST Standard Reference Materials (SRM-1546 and SRM-1849) were used to validate the ASE methods. ]ͨ#�VIr��m�2��QU��Z` Jing Xu, Dipaloke Mukherjee, Sam K.C. Find more information about Crossref citation counts. In this study ion exchange based materials were used to remove acid or base reagents in-cell without compromising the recovery of lipids. Please reconnect. Transgenic soya bean seeds accumulating β-carotene exhibit the collateral enhancements of oleate and protein content traits. Chemical Composition of Date Pits: Potential to Extract and Characterize the Lipid Fraction. %���� The new methods presented here enhance the utility of ASE and eliminate labor intensive protocols. Victor H. M. da Cruz, Rafael L. G. Priori, Patrícia D. S. Santos, Cintia S. F. Ferreira, Angélica de F. B. Piccioli, Roberta da Silveira, Jesuí V. Visentainer, Oscar O. Santos. Experimental investigation on cleaner process of enhanced fat-oil extraction from alkaline leather fleshing waste. Citations are the number of other articles citing this article, calculated by Crossref and updated daily. Extraction of Total Fat from Food Samples After Acid Hydrolysis Using Accelerated Solvent Extraction with GC-MS Analysis Brett Murphy, Brian Dorich, and Bruce Richter Thermo Fisher Scientific, Salt Lake City, UT, USA Application Note 361 Introduction Sample Valeria Nardelli, Valeria D’Amico, Francesco Casamassima, Giuseppe Gesualdo, Donghao Li, Wadir M.V. This paper describes a new in-cell method for pursuing accelerated solvent extraction (ASE) prior to lipid analysis from food samples. Accelerated Solvent Extraction (ASE) and High-Temperature Water Extraction. Find more information on the Altmetric Attention Score and how the score is calculated. Xing Liu, Xin Zhang, Yu-Zhi Rong, Jin-Hong Wu, Yong-Jian Yang, Zheng-Wu Wang. endstream endobj 51 0 obj <>>>/Filter/Standard/Length 128/O(�ռJ����6l\(lb�� �iel�Bou����)/P -1036/R 4/StmF/StdCF/StrF/StdCF/U(��S� )/V 4>> endobj 52 0 obj <>>> endobj 53 0 obj <> endobj 54 0 obj <>/ExtGState<>/Font<>/Pattern<>/ProcSet[/PDF/Text]/Properties<>>>/Rotate 0/TrimBox[0.0 0.0 594.0 792.0]/Type/Page>> endobj 55 0 obj <>stream 118 0 obj <>stream These metrics are regularly updated to reflect usage leading up to the last few days. Find more information about Crossref citation counts. Journal of Agricultural and Food Chemistry. 3 0 obj 85 0 obj <>/Encrypt 51 0 R/Filter/FlateDecode/ID[<4A7E2C81B93F6447AAD8A4D4D88F0621>]/Index[50 69]/Info 49 0 R/Length 142/Prev 186785/Root 52 0 R/Size 119/Type/XRef/W[1 3 1]>>stream endobj Development of a screening analytical method for the determination of non-dioxin-like polychlorinated biphenyls in chicken eggs by gas chromatography and electron capture detection. 50 0 obj <> endobj endstream endobj startxref 0 Li-Chun Zhao, Ying He, Xin Deng, Geng-Liang Yang, Wei Li, Jian Liang, Qian-Li Tang. 2 0 obj Marchesiello, Donatella Nardiello, Maurizio Quinto. Monica A. Schmidt, Wayne A. Parrott, David F. Hildebrand, R. Howard Berg, Amanda Cooksey, Ken Pendarvis, Yonghua He, Fiona McCarthy, Eliot M. Herman. %%EOF Critical overview of selected contemporary sample preparation techniques. the Altmetric Attention Score and how the score is calculated. <>/Font<>/XObject<>/ProcSet[/PDF/Text/ImageB/ImageC/ImageI] >>/MediaBox[ 0 0 612 792] /Contents 4 0 R/Group<>/Tabs/S/StructParents 0>> <> Get article recommendations from ACS based on references in your Mendeley library. This article is cited by <> � VR�O����Ҫ�|y�%b,����zy�X&8�E���/ѧx�G�XD�.c&v'�9� w�I��v�o����'�s���L-�*{]��~�B���LD�:��{�&tey$y!x�vd�H! Evaluation of different conventional lipid extraction techniques’ efficiency in obtaining oil from oleaginous seeds. X>. 4 0 obj 1 0 obj Rapid Determination of Fat, Protein and Amino Acid Content in Coix Seed Using Near-Infrared Spectroscopy Technique. Excellent fat recoveries were obtained for the ASE methods. <>>> x��X_o�8���Giq�E���C! Acid hydrolysis can be performed to release the bound lipids attached to protein and carbohydrates in order to enhance the extraction efficiency.

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